Alarm tag and method of making and deactivating it

ABSTRACT

This invention relates to a deactivatable tag useable with an electronic article surveillance system and comprised of planar conductive material cut into a pair of inverse, first and second spiral conductors wrapped about each other and positioned for capacitive and inductive coupling. The invention also relates to method of making tags wherein conductors are cut from a planar web of conductive material in a continuous process in a manner that the cutting results in the formation of two spiral conductors without accompanying waste of conductive material, and thereafter positioning the conductors to provide resonant circuits.

CROSS-REFERENCE TO RELATED APPLICATION

This is a continuation-in-part of copending U.S. patent application Ser. No. 06/912,466 filed Sept. 29, 1986 of S. Eugene Benge and Robert Lee Froning, now U.S. Pat. No. 4,717,438, assigned to Monarch Marking Systems, Inc.

BACKGROUND OF THE INVENTION

1. Field of the Invention

This invention relates to the art of resonant tags used in electronic article surveillance systems and to method of making such tags.

2. Brief Description of the Prior Art

The following patents are made of record: U.S. Pat. No. 3,240,647 to Morgan granted Mar. 15, 1966; U.S. Pat. No. 3,624,631 to Chomet granted Nov. 30, 1971; U.S. Pat. No. 3,810,147 to Lichtblau granted May 7, 1974; U.S. Pat. No. 3,913,219 to Lichtblau granted Oct. 21, 1975; U.S. Pat. No. 4,482,874 to Rubertus et al granted Nov. 13, 1984; U.S. Pat. No. 4,555,291 to Tait et al granted Nov. 26, 1985; U.S. Pat. No. 4,567,473 to Lichtblau granted Jan. 28, 1986; and French patent No. 2,412,923 to Degueldre.

SUMMARY OF THE INVENTION

It is an object of the invention to provide simple yet effective methods of making reliable deactivatable resonant tags for use in electronic article surveillance systems.

It is an object of the invention to provide improved, reliable, deactivatable resonant tags which can be made on a production basis.

According to the invention, there is provided a method of making a deactivatable tag which includes the steps of providing a resonant circuit responsive to receipt of a first energy level signal to emit an alarm signal to indicate the presence of the resonant circuit in an interrogation zone, the circuit including an inductor having a spiral conductor, and providing an activatable connection to the spiral conductor including normally non-conductive material which can be rendered conductive in response to a second energy level signal at an energy level higher than the first energy level signal. It is preferred that the step of providing the activatable connection includes the step of applying the normally non-conductive material between spaced but connected portions of the spiral conductor.

One specific embodiment includes the steps of coating or printing a normally non-conductive but activatable conductor-containing material onto a support so as to extend across two and preferably all the turns of the spiral conductor and thereafter coating or printing a conductive material over the normally non-conductive material in electrically isolated relationship to the spiral conductor. When the tag is put into use, it can be deactivated by subjecting the resonant circuit to the second energy level signal. The second energy level signal changes the normally non-conductive material into a conductive material.

Another specific embodiment includes the step of positioning a web of conductive material adjacent one of the spiral conductors, with the conductive material web having a layer of a normally non-conductive material electrically isolating the conductive material web from the spiral conductor, wherein the normally non-conductive material can be rendered conductive in response to the second energy level signal.

Another specific embodiment includes the steps of providing a resonant circuit responsive to receipt of a first energy level signal to emit an alarm signal to indicate the presence of the resonant circuit in an interrogation zone, and positioning an insulated conductor having a breakdown coating in contact with the circuit for deactivating the tag in response to a second energy level signal at an energy level higher than the first energy level signal.

BRIEF DESCRIPTION OF THE DRAWINGS

FIG. 1 is an exploded perspective view of a tag in accordance with an embodiment of the invention;

FIG. 2 is a fragmentary sectional view of the tag shown in FIG. 1;

FIG. 3 is a diagrammatic perspective view illustrating method of making a tag in accordance with the invention;

FIG. 4 is a diagrammatic top plan view showing a mask having been applied to a first adhesive coated web and showing an electrically conductive web being laminated to the masked first adhesive coated web;

FIG. 5 is a diagrammatic top plan view showing the conductive web having been cut to provide first and second pairs of conductors and showing a masked second adhesive coated web being laminated to the conductive web;

FIG. 6 is a diagrammatic top plan view showing the first coated web with the first conductors adhered thereto being separated relative to the second coated web with the second conductors adhered thereto, and showing further the first coated web having been recoated with adhesive and two webs of dielectric being laminated to the recoated first coated web, and showing the dielectric webs having been coated with adhesive;

FIG. 7 is a diagrammatic top plan view showing the second coated web with the second conductors adhered thereto having been shifted and laminated over and to the dielectric webs and to the first coated web with the first conductors to provide a composite tag web, showing the staking of the first and second conductors of each tag to provide resonant circuits for each tag, and showing slitting of the composite tag web to provide a plural series of composite tag webs;

FIG. 8 is a vertically exploded view showing the first and second coated webs with the first and second conductors that result from cutting the electrically conductive web spirally;

FIG. 9 is a top plan view showing the first and second coated webs shifted by a distance equal to the width of one conductor spiral plus the width of one conductor;

FIG. 10 is a top plan view of two tags with the dielectric web shown in phantom lines;

FIG. 11 is a fragmentary perspective view which, when taken together with the preceding figures of the drawings, illustrates an improved method of making deactivatable tags;

FIG. 12 is a fragmentary top plan view taken along line 12--12 of FIG. 11;

FIG. 13 is a sectional view taken along line 13--13 of FIG. 12;

FIG. 14 is a fragmentary perspective view similar to FIG. 1, but showing one embodiment of structure for deactivating the tag;

FIG. 15 is a fragmentary top plan view of the tag shown in FIG. 14;

FIG. 16 is a fragmentary perspective view which, taken together with FIGS. 1 through 10, illustrated an alternative improved method of making deactivatable tags;

FIG. 17 is a fragmentary top plan view taken along line 17--17 of FIG. 16;

FIG. 18 is a sectional view taken along line 18--18 of FIG. 17;

FIG. 19 is a fragmentary perspective view similar to FIG. 14 but showing another embodiment of structure for deactivating the tag;

FIG. 20 is a fragmentary top plan view of the tag shown in FIG. 19; and

FIG. 21 is a sectional view similar to FIG. 18 but showing an alternative structure for deactivating the tag.

DESCRIPTION OF THE PREFERRED EMBODIMENTS

Referring initially to FIG. 1, there is shown an exploded view of a tag generally indicated at 19. The tag 19 is shown to include a sheet 20T having pressure sensitive adhesive 21 and 22 on opposite faces thereof. A mask 23 in a spiral pattern covers a portion of the adhesive 21 and a release sheet 24T is releasably adhered to the adhesive 22. The mask 23 renders the adhesive 21 which it covers non-tacky or substantially so. A conductor spiral indicated generally at 25 includes a spiral conductor 26 having a number of turns. The conductor 26 is of substantially the same width throughout its length except for a connector bar 27 at the outer end portion of the conductor spiral 26. There is a sheet of dielectric 28T over and adhered to the conductor spiral 25 and the underlying sheet 20T by means of adhesive 29. A conductor spiral generally indicated at 30 includes a spiral conductor 31 having a number of turns. The conductor 31 is adhered to adhesive 29 on the dielectric 28T. The conductor 31 is substantially the same width throughout its length except for a connector bar 32 at the outer end portion of the conductor spiral 30. The conductor spirals 25 and 30 are generally aligned in face-to-face relationship except for portions 33 which are not face-to-face with the conductor 26 and except for portions 35 which are not face-to-face with the conductor 31. A sheet 37T has a coating of a pressure sensitive adhesive 38 masked off in a spiral pattern 39. The exposed adhesive 38' is aligned with the conductor spiral 30. Adhesive is shown in FIG. 1 by heavy stippling and the masking is shown in FIG. 1 by light stippling with cross-hatching. The connector bars 27 and 32 are electrically connected, as for example by staking 90. It should be noted that the staking 90 occurs where connector bars 27 and 32 are separated only by adhesive 29. There is no paper, film or the like between the connector bars 27 and 32. Accordingly, the staking disclosed in the present application is reliable.

With reference to FIG. 3, there is shown diagrammatically a method for making the tag 19 shown in FIGS. 1 and 2. A roll 40 is shown to be comprised of a composite web 41 having a web 20 with a full-gum or continuous coatings of pressure sensitive adhesive 21 and 22 on opposite faces thereof. The web 20 is "double-faced" with adhesive. A release liner or web 42 is releasably adhered to the upper side of the web 20 by the pressure sensitive adhesive 21, and the underside of the web 20 has a release liner or web 24 releasably adhered to the pressure sensitive adhesive 22. As shown, the release liner 42 is delaminated from the web 20 to expose the adhesive 21. The adhesive coated web 20 together with the release liner 24 pass partially about a sandpaper roll 43 and between a pattern roll 44 and a back-up roll 45 where mask patterns 23 are applied onto the adhesive 21 to provide longitudinally recurring adhesive patterns 21'. Masking material from a fountain 46 is applied to the pattern roll 44. With reference to FIG. 4, the portion marked A represents the portion of the web 20 immediately upstream of the pattern roll 44. The portion marked B shows the mask patterns 23 printed by the roll 44. The patterns 23 are represented by cross-hatching in FIG. 4. With reference to FIG. 3, the web 20 now passes through a dryer 47 where the mask patterns 23 are dried or cured. The adhesive 21 is rendered non-tacky at the mask patterns 23. A web 49 of planar, electrically conductive material such as copper or aluminum from a roll 48 is laminated onto the coated web 20 as they pass between laminating rolls 50 and 50'. Reference character C in FIG. 4 denotes the line where lamination of the webs 20 and 49 occurs. With reference to FIG. 3, the laminated webs 20 and 49 now pass between a cutting roll 51 having cutting blades 52 and a back-up roll 53. The blades 52 cut completely through the conductive material web 49 but preferably do not cut into the web 20. The blades 52 cut the web 49 into a plurality of series of patterns 25 and 30 best shown in the portion marked D in FIG. 5. With reference again to FIG. 3, there is shown a roll 54 comprised of a composite web 55 having a web 37 with a full-gum or continuous coating of pressure sensitive adhesive 38 and a release liner 56 releasably adhered to the adhesive 38 on the web 37. The release liner 56 is separated from the web 37 and the web 37 passes about a sandpaper roll 57. From there the web 37 passes between a pattern roll 58 and a back-up roll 59 where mask patterns 39 are applied onto the adhesive 38 to render the adhesive 38 non-tacky at the mask patterns 39 to provide longitudinally recurring adhesive patterns 38' (FIG. 1). Masking material from a fountain 60 is applied to the pattern roll 58. The masking material of which the patterns 23 and 39 are comprised is a commercially available printable adhesive deadener such as sold under the name "Aqua Superadhesive Deadener" by Environmental Inks and Coating Corp, Morganton, N.C. From there the web 37 passes partially about a roll 61 and through a dryer 62 where the mask patterns 39 are dried or cured. The adhesive 38 is rendered non-tacky at the mask patterns 39. From there the webs 20, 49 and 37 pass between laminating rolls 63 and 64. FIG. 5 shows that lamination occurs along line E where the web 37 meets the web 49. When thus laminated, each adhesive pattern 21' registers only with an overlying conductor spiral 25 and each adhesive pattern 38' registers only with an underlying conductor spiral 30.

The webs 20, 37 and 49 pass successively partially about rolls 65 and 66 and from there the web 37 delaminates from the web 20 and passes partially about a roll 67. At the place of delamination, the web 49 separates into two webs of conductor spirals 25 and 30. As shown in FIG. 6, delamination occurs along the line marked F. When delamination occurs, the conductor spirals 30 adhere to the adhesive patterns 38' on the web 37, and the conductor spirals 25 adhere to the adhesive patterns 21' on the web 20. Thus, the conductor spirals 30 extend in one web and the spirals 25 extend in another web. The web 20 passes partially about rolls 68, 69 and 70 and from there pass between an adhesive coating roll 71 and a back-up roll 72. Adhesive 29 from a fountain 73 is applied to the roll 71 which in turn applies a uniform or continuous coating of adhesive 29 to the web 20 and over conductive spirals 25. The portion marked G in FIG. 6 shows the portion of the web 20 and conductor spirals 25 between the spaced rolls 66 and 72. The portion marked H shows the portion of the web 20 between the spaced rolls 72 and 74. With reference to FIG. 3, the web 20 passes through a dryer 75 where the adhesive 29 is dried. A plurality, specifically two laterally spaced dielectric webs 28a and 28b wound in rolls 76 and 77 are laminated to the web 20 as the webs 20, 28a and 28b pass between the rolls 74 and 74'. This laminating occurs along reference line I indicated in FIG. 6. With reference to FIG. 3, the web 20 with the conductor spirals 25 and the dielectric webs 28a and 28b pass about rolls 78 and 79 and pass between an adhesive applicator roll 80 and a back-up roll 81. The roll 80 applies adhesive 29' received from a fountain 83 to the webs 28a and 28b and to the portions of the web 20 not covered thereby. From there, the webs 20, 28a and 28b pass through a dryer 84 and partially about a roll 85.

The web 37 which had been separated from the web 20 is laminated at the nip of laminating rolls 86 and 87 along a line marked J in FIG. 7 to provide a composite tag web generally indicated at 88. The webs 20, 28a, 28b and 37 are laminated between rolls 86 and 87 after the conductor spirals 30 have been shifted longitudinally with respect to the conductor spirals 25 so that each conductor spiral 30 is aligned or registered with an underlying conductor spiral 25. The shifting can be equal to the pitch of one conductor spiral pattern as indicated at p (FIG. 9) plus the width w of one conductor, or by odd multiples of the pitch p plus the width w of one conductor. Thus, each pair of conductor spirals 25 and 30 is capable of making a resonant circuit detectable by an appropriate article surveillance circuit.

FIG. 8 shows the web 20 and the web 37 rotated apart by 180°. FIG. 9 shows the web 20 and the web 37 rotated apart by 180° and as having been shifted with respect to each other so that the conductor spirals 25 and 30 are aligned. As best shown in FIG. 10, the dielectric 28a terminates short of stakes 90 resulting from the staking operation. By this arrangement the stakes 90 do not pass through the dielectric 28a (or 28b). FIG. 10 shows the conductor spirals 25 and 30 substantially entirely overlapped or aligned with each other, except as indicated at 35 for the conductor spiral 25 and as indicated at 33 for the conductor spiral 30. Each circuit is completed by staking the conductor bars 27 and 32 to each other as indicated at 90 or by other suitable means. The staking 90 is performed by four spiked wheels 89 which make four stake lines 90 in the composite web 88. The spiked wheels 89 pierce through the conductor bars 27 and 32 and thus bring the conductor bars 27 and 32 into electrically coupled relationship. The web composite 88 is slit into a plurality of narrow webs 91 and 92 by slitter knife 93 and excess material 94 is trimmed by slitter knives 95. The webs 91 and 92 are next cut through up to but not into the release liner 24 by knives on a cutter roll 96, unless it is desired to cut the tags T into separated tags in which event the web 88 is completely severed transversely. As shown, the webs 91 and 92 continue on and pass about respective rolls 97 and 98 and are wound into rolls 99 and 100. As shown in FIG. 7, the staking 90 takes place along a line marked K and the slitting takes place along a line marked L.

The sheet 37T, the dielectric 28T, the sheet 20T and the sheet 24T are respectively provided by cutting the web 37, the web 28a (or 28b), the web 20 and the web 24.

FIG. 11 is essentially a duplicate of a portion of FIG. 3, but a pair of coating and drying stations generally indicated at 111 and 112 where respective coatings 113 and 114 in the form of continuous stripes are printed and dried. The coating 113 is conductive and is applied directly onto the pressure sensitive adhesive 38 on the web 37. The coatings 114 are wider than the respective coatings 113 which they cover to assure electrical isolation, as best shown in FIGS. 12 and 13. The coatings 114 are composed of a normally non-conductive activatable material. The remainder of the process is the same as the process taught in connection with FIGS. 1 through 10.

With reference to FIGS. 14 and 15, there is shown a fragment of the finished tag 37T' with the coatings 113 and 114 having been severed as the tag 37T' is severed from the tag web as indicated at 113T and 114T respectively. As shown the coating 113T is of constant width and thickness throughout its length and the coating 114T is of constant width and thickness but is wider than the coating 113T. The coating 113T which is conductive is thus electrically isolated from the conductor spiral 30. The coatings 113T and 114T comprise an activatable connection AC which can be activated by subjecting the tag to a high level of energy above that for causing the resonant circuit to be detected at an interrogation zone.

FIG. 16 is essentially a duplicate of a portion of FIG. 3, but a pair of webs 118 and 119 are adhered to the adhesive 38 on the web 37. The webs 118 and 119 are wound onto spaced reels 120 and 121. The webs 118 and 119 pass from the reels 120 and 121 partially about a roll 122. The webs 118 and 119 are spaced apart from each other and from the side edges of the web 37. The webs 118 and 119 are identical in construction, and each includes a thin layer of conductive material 123 such as copper or aluminum on a layer of paper 123', a high temperature, normally non-conductive, activatable, conductor-containing layer 124, and a low temperature, normally non-conductive, activatable, conductor-containing layer 125. The layers 124 and 125 contain conductors such as metal particles or encapsulated carbon. The layer 125 bonds readily when heated, so a drum heater 115 is positioned downstream of the roll 67 (FIGS. 3 and 16) and upstream of the rolls 86 and 87 (FIG. 3). The heated circuits 30, heat the layer 125 and a bond is formed between the circuits 30 and the layer 125. Rolls 116 and 117 (FIG. 16) guide the web 37 about the drum heater 115. The heating of the layer 125 has some tendency to break down the normally non-conductive nature of the layer 125, but this is not serious because the layer 124 is not broken down or activated by heat from the drum heater 115.

With reference to FIGS. 19 and 20, there is shown a fragment of a finished tag 37T" with the webs 118 and 119 having been severed so as to be coextensive with the tag 37T" and is indicated at 118T. The web strip or stripe 118T includes the paper layer 123', the conductive layer or conductor 123 and the normally non-conductive layers 124 and 125. The layers 123, 124 and 125 are shown to be of the same width and comprise an activatable connection AC. Both coatings 124 and 125 electrically isolate the conductor 123 form the conductor spiral 30. In other respects the tag 37T" is identical to the tag 37T and is made by the same process as depicted for example in FIG. 3.

The embodiment of FIG. 21 is identical to the embodiment of FIGS. 16 through 20 except that instead of the webs 118 and 119 there are a pair of webs comprised of flat bands, one of which is shown in FIG. 21 and is depicted at 118'. The band 118' is comprised of a web or band conductor 126 of a conductive material such as copper enclosed in a thin coating of a non-conductive material 127. The band 118' comprises an activatable connection AC. As seen in FIG. 21, the upper surface of the coating 127 electrically isolates the conductor 126 from the conductor spiral 30. The band 118' is processed according to one specific embodiment, by starting with coated motor winding wire, Specification No. 8046 obtained from the Belden Company, Geneva, Ill. 60134 U.S.A. and having a diameter of about 0.004 inch with an insulating coating of about 0.0005, flattening the wire between a pair of rolls into a thin band having a thickness of 0.0006 inch. Thus processed, the insulating coating is weakened to a degree which breaks down when the resulting tag is subjected to a sufficiently high energy level signal. The coating 118' is thus termed a "breakdown coating" because it acts as an insulator when the tag is subjected to an interrogation signal at a first energy level but no longer acts as an electrical insulator when subjected to a sufficently higher energy level signal. The conductor 126 accordingly acts to short out the inductor 30 at the higher energy level signal.

The embodiments depicted in FIGS. 11 through 20 and described in connection therewith enable the tag 37T' or 37T" to be detected in an interrogation zone when subjected to a radio frequency signal at or near the resonant frequency of the resonant circuit. By sufficiently increasing the energy level of the signal, the normally non-conductive coating 114 (or 114T), or 124 and 125 becomes conductive to alter the response of the resonant circuit. This is accomplished in a specific embodiment by using a normally non-conductive coating to provide an open short-circuit between different portions of the conductor spiral 30.

When the tag is subjected to a high level of energy, in the embodiments of FIGS. 11 through 15, and 16 through 20 the normally non-conductive coating becomes conductive and shorts out the inductor. Thus, the resonant circuit is no longer able to resonate at the proper frequency and is unable to be detected by the receiver in the interrogation zone.

While the illustrated embodiments disclose the activatable connection AC provided by an additional conductor as extending across all the turns of the conductor spiral 30 and by a normally non-conductive material or breakdown insulation electrically isolating the conductor from the conductor spiral 30 and also extending across all of the turns of the conductor sprial 30, the invention is not to be considered limited thereby.

By way of example, not limitation, examples of the various coatings are stated below:

    ______________________________________                                         I. For the embodiment of FIGS. 11 through 15                                   A.   Examples of the normally non-conductive                                        coating 114 are:                                                          Example 1            Parts by Weight                                           ______________________________________                                         cellulose acetate (C.A.)                                                                            60                                                        powder (E-398-3)                                                               acetone              300                                                       ______________________________________                                         Mixing procedure: Solvate C.A. powder in                                       acetone with stirring.                                                         C.A./copper dispersion                                                                              15                                                        above C.A. solution (16% T.S.)                                                 copper 8620 powder   2.5                                                       Mixing procedure: Add copper powder to                                         C.A. solution with adequate stirring to                                        effect a smooth metallic dispersion.                                           Example 2                                                                      ______________________________________                                         acrylvid B-48N       30                                                        (45% in toluene)                                                               acetone              20                                                        isopropanol          3                                                         Above solution (25% T.S.)                                                                           10                                                        copper 8620 powder   5                                                         ______________________________________                                         Mixing procedure: disperse copper powder                                       into B-48N solution (Percent copper powder                                     is 60-70% on dry weight basis.)                                                B.   Examples of the conductive coating 113 are:                               Example 1            Parts by Weight                                           ______________________________________                                         acryloid B-67 acrylic                                                                               25                                                        (45% in naptha)                                                                naptha               16                                                        silflake #237 metal powder                                                                          42                                                        ______________________________________                                         Mixing procedure: add metal powder to                                          solvent and wet out. Add solvated acrylic                                      and stir well to disperse. Mix or shake                                        well prior to use. (75% to 85% conductive                                      metal on dry weight basis.)                                                     Example 2                                                                     ______________________________________                                         acryloid NAD-10      10                                                        (40% in naptha)                                                                silflake #237 metal powder                                                                          20                                                        ______________________________________                                         Mixing procedure: Add metal powder to                                          acrylic dispersion with stirring.                                              Example 3                                                                      ______________________________________                                         S & V aqueous foil ink                                                                              5                                                         OFG 11525 (37% T.S.)                                                           silflake #237 metal powder                                                                          8                                                         ______________________________________                                         Mixing procedure: Add metal powder to                                          aqueous dispersion slowly with adequate                                        agitation to effect a smooth metallic                                          dispersion.                                                                    I. For the embodiment of FIGS. 16 through 20                                   A.   Examples of the low temperature coating 125                                    are:                                                                      Example 1            Parts by Weight                                           ______________________________________                                         acryloid NAD-10 dispersion                                                                          10                                                        (30% T. Solids)                                                                naptha               2                                                         copper 8620 copper powder                                                                           5                                                         ______________________________________                                         Mixing procedure: wet copper powder with                                       Naptha and disperse completely. Add NAD-10                                     dispersion slowly with stirring. Mix well                                      or shake before use.                                                           Example 2                                                                      ______________________________________                                         polyester resin      28                                                        (K-1979)                                                                       ethanol              10                                                        isopropanol          10                                                        ethyl acetate        20                                                        above polyester solution                                                                            10                                                        copper 8620 powder   2.5                                                       ______________________________________                                         Mixing procedure: add copper powder to                                         polyester solution while stirring to effect                                    a smooth metallic dispersion.                                                  (48% copper powder on dry basis)                                               B.   Examples of the high temperature coating                                       124 are:                                                                  Example 1                                                                      ______________________________________                                         cellulose acetate butyrate                                                                          40                                                        (C.A.B.)(551-0.2)                                                              toluene              115                                                       Ethyl Alcohol        21                                                        Above C.A.B. solution                                                                               10                                                        (22.7%)                                                                        toluene              2                                                         copper 8620 copper powder                                                                           5                                                         ______________________________________                                         Mixing procedure: wet copper powder with                                       solvent and add C.A.B. solution with                                           stirring.                                                                      Example 2                                                                      ______________________________________                                         acryloid B-48N       30                                                        (45% in toluene)                                                               acetone              20                                                        isopropanol          3                                                         Above solution (25% T.S.)                                                                           10                                                        copper 8620 copper powder                                                                           5                                                         (Dry weight basis -- copper                                                    is 60-70%)                                                                     ______________________________________                                         Mixing procedure: add copper powder to                                         above solution with proper agitation to                                        effect a smooth metallic dispersion.                                           ______________________________________                                    

The materials used in the above examples are obtainable from the following suppliers:

Acryloid NAD-10, Acryloid B-48N and Acryloid B-67, Rohm & Hass, Philadelphia, Pa.;

Cellulose Acetate (E-398-3) and Cellulose Acetate Butyrate (551-0.2), Eastman Chemical Products, Inc., Kingsport, Tenn.;

Copper 8620, U.S. Bronze, Flemington, N.J.;

Silflake #237, Handy & Harmon, Fairfield, Conn.;

Krumbhaar K-1979, Lawter International, Inc., Northbrook, Ill.;

Aqeuous foil ink OFG 11525, Sinclair & Valentine, St. Paul, Minn.

Other embodiments and modifications of the invention will suggest themselves to those skilled in the art, and all such of these as come within the spirit of this invention are included within its scope as best defined by the appended claims. 

We claim:
 1. Method of making a deactivatable tag for use in an electronic article surveillance system, comprising the steps of: providing a resonant circuit responsive to receipt of a first energy level signal to emit an alarm signal to indicate the presence of the resonant circuit in an interrogation zone, the circuit including an inductor having a spiral conductor, providing an additional conductor, and positioning the additional conductor adjacent the resonant circuit while electrically isolating the additional conductor from the spiral conductor by a normally non-conductive material which can be rendered conductive to deactivate the tag in response to a second energy level signal at an energy level higher than the first energy level signal.
 2. Method of deactivating a tag made by the method defined in claim 1, further including the steps of applying the second energy level signal to the tag to render the non-conductive material conductive so that the additional conductor alters the characteristics of the inductor and hence the circuit to prevent the emission of the alarm signal.
 3. Method of making a deactivatable tag for use in an electronic article surveillance system, comprising the steps of: providing a resonant circuit responsive to receipt of a first energy level signal to emit an alarm signal to indicate the presence of the resonant circuit in an interrogation zone, the circuit including an inductor having a spiral conductor, applying a first coating across at least a portion of the spiral conductor with the first coating being normally non-conductive but which can be rendered conductive in response to a second energy level signal at an energy level higher than the first energy level signal, and applying a conductive second adjacent the resonant circuit and coating over the first coating in electrically isolated relationship to the spiral conductor so that upon receipt of the second energy level signal the first coating becomes conductive and the second coating thereby becomes electrically coupled to the conductor to alter the characteristics of the inductor to prevent emission of the alarm signal.
 4. Method of making a deactivatable tag for use in an electronic article surveillance system, comprising the steps of: providing a resonant circuit responsive to receipt of a first energy level signal to emit an alarm signal to indicate the presence of the circuit in an interrogation zone, the circuit including an inductor having a spiral conductor with a plurality of turns, providing an open short-circuit between two turns of the spiral conductor, the step of providing the open short-circuit including the step of isolating the two turns from each other by a normally non-conductive material disposed adjacent the resonant circuit and which can be rendered conductive to short circuit the inductor in response to receipt of a second energy level signal at an energy level higher than the first energy level signal.
 5. Method of making a deactivatable tag for use in an electronic article surveillance system, comprising the steps of: providing a resonant circuit responsive to receipt of a first energy level signal to emit an alarm signal to indicate the presence of the resonant circuit in an interrogation zone, the circuit including an inductor having a spiral conductor with a plurality of turns, providing an open short-circuit between two turns of the spiral conductor, the step of providing the open short-circuit including the step of applying a first coating across at least a portion of one of the turns with the first coacting being normally non-conductive but which can be rendered conductive in response to a second energy level signal at an energy level higher than the first energy level signal, and applying a conductive second coating adjacent the resonant circuit and between the two turns and over the first coating and normally electrically isolated from the two turns so that upon receipt of the second energy level signal the inductor is short-circuited and consequently the characteristics of the inductor are altered to prevent emission of the alarm signal.
 6. Method of making a deactivatable tag for use in an electronic article surveillance system, comprising the steps of: providing a resonant circuit responsive to receipt of a first energy level signal to emit an alarm signal to indicate the presence of the circuit in an interrogation zone, the circuit including an inductor having a spiral conductor with a plurality of turns, and positioning a web of conductive material adjacent the resonant circuit, with the conductive material web having a layer of a normally non-conductive material electrically isolating the conductive material web from one of the spiral condutors but wherein the normally non-conductive material can be rendered conductive in response to a second energy level signal at an energy level higher than the first energy level signal to alter the characteristics of the inductor to prevent emission of the alarm signal.
 7. Method of making a deactivatable tag for use in an electronic article surveillance system, comprising the steps of: providing a first web with a first series of first spiral conductors and a second web with a series of second spiral conductors, providing a web of conductive material having a layer of normally non-conductive material, positioning the conductive material web with the normally non-conductive layer adjacent either the first or the second series of conductors, adhering the first and second webs to each other, connecting the conductors of the first and second webs to each other to provide a series of resonant circuits in a composite web, wherein the step of positioning the web of conductive material includes disposing the conductive material adjacent the resonant circuit but normally isolated from the resonant circuit by the normally non-conductive layer, separating the composite web into tags each having a resonant circuit, and wherein the normally non-conductive layer can be rendered conductive in response to an energy level higher than that level necessary to activate the tag.
 8. Method of making a deactivatable tag for use in an electronic article surveillance system, comprising the steps of: providing a first web, printing conductive material on the first web, printing non-conductive material on the first web over the conductive material, providing a second web, first and second spiral conductors positioned between the first and second webs, adhering the webs to each other with pairs of the first and second spiral conductors connected to provide resonant circuits, wherein the normally non-conductive material can be rendered conductive in response to an energy level higher than that level necessary to activate the tag, and separating the webs to provide tags each having a deactivatable circuit, and with the non-conductive material normally electrically isolating the conductive material from the resonant circuit.
 9. Method of making a deactivatable tag for use in an electronic article surveillance system, comprising the steps of: providing a resonant circuit responsive to receipt of a first energy level signal to emit an alarm signal to indicate the presence of the resonant circuit in an interrogation zone, the circuit including an inductor having a spiral conductor, and providing an activatable connection adjacent to the resonant circuit including normally non-conductive, conductor-containing material which can be rendered conductive in response to a second energy level signal at an energy level higher than the first energy level signal, and with the conductor in the conductor containing material being normally electrically isolated from the resonant circuit.
 10. Method as defined in claim 9, wherein the step of providing an activatable connection includes the step of applying the normally non-conductive material between spaced but connected portions of the spiral conductor.
 11. Method as defined in claim 9, wherein the step of providing an activatable connection includes the step of connecting spaced portions of the spiral conductor with an additional conductor electrically isolated from the spaced portions by the normally non-conductive material.
 12. A deactivatable tag for use in an electronic article surveillance system, the tag comprising: a resonant circuit responsive to receipt of a first energy level signal to emit an alarm signal to indicate the presence of the resonant circuit in an interrogation zone, the resonant circuit including a spiral conductor, a deactivating conductor adjacent the resonant circuit and adapted to connect spaced portions of the spiral conductor to each other, normally non-conductive material electrically isolating the deactivating conductor from at least one portion of the spiral conductor, and wherein the normally non-conductive material can be rendered conductive to deactivate the resonant circuit in response to a second energy level signal higher than the first energy level signal.
 13. Method of making a deactivatable tag for use in an electronic article surveillance system, comprising the steps of: providing a resonant circuit responsive to receipt of a first energy level signal to emit an alarm signal to indicate the presence of the resonant circuit in an interrogation zone, and positioning an insulated conductor having a breakdown coating in contact with the resonant circuit for deactivating the tag in response to a second energy level signal at an energy level higher than the first energy level signal, with the breakdown coating normally electrically isolating the conductor from the resonant circuit.
 14. Method as defined in claim 13, wherein the insulated conductor is made by flattening an insulated conductive metal wire.
 15. A deactivatable tag for use in an electronic article surveillance system, the tag comprising: a resonant circuit responsive to receipt of a first energy level signal to emit an alarm signal to indicate the presence of the resonant circuit in an interrogation zone, the resonant circuit including a spiral conductor having turns, a stripe of normally non-conductive material across at least two turns, a stripe of conductive material adjacent the resonant circuit and normally electrically isolated from the two turns by the normally non-conductive material, and wherein the normally non-conductive material can be rendered conductive to deactivate the resonant circuit in response to a second energy level signal higher than the first energy level signal.
 16. A deactivatable tag as defined in claim 15, wherein the stripe extends across all the turns of the spiral conductor.
 17. A deactivatable tag for use in an electronic article surveillance system, the tag comprising: a resonant circuit responsive to receipt of a first energy level signal to emit an alarm signal to indicate the presence of the resonant circuit in an interrogation zone, the resonant circuit including a spiral conductor, means adjacent the resonant circuit for altering the signal emitted by the resonant circuit to prevent detection of the presence of the circuit in the interrogation zone, the signal altering means including normally non-conductive conductor-containing material connected to the spiral conductor, wherein the conductor in the material of the altering means is normally electrically isolated from the resonant circuit and wherein the material can be rendered conductive in response to a second energy level signal at an energy level higher than the first energy level signal.
 18. A deactivatable tag as defined in claim 17, wherein the signal altering means further includes conductive material electrically isolated from the spiral conductor by the normally non-conductive material.
 19. A deactivatable tag as defined in claim 17, wherein the spiral conductor includes a plurality of turns, the normally non-conductive material constituting a stripe across at least two of the turns, a stripe of conductive material on the normally non-conductive material stripe and across the same two turns, and wherein the stripe of conductive material is electrically isolated from those two turns by the normally non-conductive material stripe.
 20. A deactivatable tag as defined in claim 19, wherein both the normally non-conductive material stripes and the conductive material stripe extend across all the turns of the spiral conductor.
 21. A deactivatable tag for use in an electronic article surveillance system, the tag comprising: a resonant circuit responsive to a first energy level signal to emit an alarm signal to indicate the presence of the resonant circuit in an interrogation zone, and an insulated conductor adjacent the resonant circuit and having a breakdown coating in contact with the circuit for deactivating the tag in response to a second energy level signal at an energy level higher than the first energy level signal, with the breakdown coating normally electrically isolating the conductor from the resonant circuit. 